HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-o-phenylenediamine → HCID 178488051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-o-phenylenediamine | HCID 153404 | — |
| Reactant | HCID 131721827 | HCID 131721827 | — |
| Product | HCID 178488051 | HCID 178488051 | — |
Reaction Steps
Prepared from 8-methoxy-2-trifluoromethylquinoline-5-carbonyl choride, hydrochloride (Intermediate 35 of PCT/GB97/01359) and 4-methoxy-1,2-phenylenediamine; purification by column chromatography eluting with 50%-70% ethyl acetate in hexane afforded the title compound as a pale yellow solid (1.32 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06069151 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-796c3244dd82459ba9c73d2e4292426a |
| Source note | uspto-grants-2000_05 |