Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1108621Generated: October 29, 2026

HCID 18783934, compound → 2-(Dimethylamino)ethyl alpha-hydroxy-alpha-phenylbenzeneacetate

https://huagongshe.com/reaction/1108621

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18783934HCID 18783934—
ReactantHCID 70284302HCID 70284302—
Product2-(Dimethylamino)ethyl alpha-hydroxy-alpha-phenylbenzeneacetateHCID 13768—

Reaction Steps

0.24 g (0.802 mmol) of o-(2-dimethylaminoethyl)benzilic acid shown below was obtained as a faint yellow solid from 0.31 g (1.0 mmol) of methyl o-(2-dimethylaminoethyl)benzilate in the same manner as in Production Example 2 (4). ##STR24## Its spectroscopic data are as follows: 1H-NMR (CDCl3) δ (ppm) : 2.87 (6H, s), 3.09 (2H, t, J=4.8 Hz), 3.51 (2H, t, J=4.8 Hz), 7.21~7.30 (6H, m), 7.50~7.54 (4H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06069149
Source datasetuspto-grants-2000_05
ORD IDord-5b5014e8840f45aba6724bb3ba4489c2
Source noteuspto-grants-2000_05