HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18783934, compound → 2-(Dimethylamino)ethyl alpha-hydroxy-alpha-phenylbenzeneacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18783934 | HCID 18783934 | — |
| Reactant | HCID 70284302 | HCID 70284302 | — |
| Product | 2-(Dimethylamino)ethyl alpha-hydroxy-alpha-phenylbenzeneacetate | HCID 13768 | — |
Reaction Steps
0.24 g (0.802 mmol) of o-(2-dimethylaminoethyl)benzilic acid shown below was obtained as a faint yellow solid from 0.31 g (1.0 mmol) of methyl o-(2-dimethylaminoethyl)benzilate in the same manner as in Production Example 2 (4). ##STR24## Its spectroscopic data are as follows: 1H-NMR (CDCl3) δ (ppm) : 2.87 (6H, s), 3.09 (2H, t, J=4.8 Hz), 3.51 (2H, t, J=4.8 Hz), 7.21~7.30 (6H, m), 7.50~7.54 (4H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06069149 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-5b5014e8840f45aba6724bb3ba4489c2 |
| Source note | uspto-grants-2000_05 |