HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18784135, compound → HCID 18784188, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18784135 | HCID 18784135 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18784188 | HCID 18784188 | — |
Reaction Steps
N-Benzyl-N-[3-(4-methoxyphenyl)cyclopentylmethyl]amine (free compound, 5.60 g) was dissolved in ethyl acetate (100 ml), 4 N HCl-ethyl acetate solution (10 ml) was added, and the mixture was stirred at room temperature for 2 hours. The deposited crystals were filtered and air-dried to give 6.30 g of N-benzyl-N-[3-(4-methoxyphenyl) cyclopentylmethyl]amine hydrochloride (quantitative yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06069176 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-f718532fe9284514b30dc11558683c2e |
| Source note | uspto-grants-2000_05 |