Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trimethoxysilane | HCID 17215 | — |
| Reactant | HCID 54551299 | HCID 54551299 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54568787 | HCID 54568787 | 36% |
Reaction Steps
Into a 100 mL round bottom flask were added 9.17 grams (0.07 mol) of 1-(1-propenoxy)-2-vinyloxyethane, 3 mg of (PPh3)3RuCl2, 11.3 grams of (MeO)3SiH (0.09 mol), and 15 ml of dried toluene. The resulting purple solution was refluxed at 85° C. for 12 hours. Fractional vacuum distillation yielded 1-(1-propenoxy)-2(2-trimethoxysilylethoxy)ethane (V) in 36% yield as a colorless liquid, b.p. 70° C./0.15 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06069259 |
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| Source dataset | uspto-grants-2000_05 |
|---|
| ORD ID | ord-3b019b93be824e5d86e1fcbe26ab4875 |
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| Source note | uspto-grants-2000_05 |
|---|
