HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)benzoyl chloride → HCID 19021184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)benzoyl chloride | HCID 67607 | — |
| Reactant | 4-(5-Nonyl-2-pyrimidinyl)phenol | HCID 135824745 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19021184 | HCID 19021184 | — |
Reaction Steps
0.01 m of p-(trifluoromethyl)-benzoyl chloride is added dropwise with stirring to a solution of 0.01 m of 2-p-hydroxyphenyl-5-nonylpyrimidine in 20 ml of pyridine at 0°-5°, the mixture is stirred for 20 hours at room temperature, and worked up as usual. p-(5-Nonylpyrimidin-2-yl)-phenyl p-(trifluoromethyl)-benzoate is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05318721 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-74c3ba9508f54063a3c831a0898fc7a7 |
| Source note | uspto-grants-1994_06 |