HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 1-phenyl-7-chloro-3-(1H-1,2,4-triazol-1-ylmethyl)-2(1H)-quinolone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 7-chloro-1-phenyl-3-chloromethyl-2(1H)-quinolone | HCID 19021630 | — |
| Reactant | HCID 178507080 | HCID 178507080 | — |
| Product | 1-phenyl-7-chloro-3-(1H-1,2,4-triazol-1-ylmethyl)-2(1H)-quinolone | HCID 19021637 | — |
Reaction Steps
Following the procedure of example 22, react 7-chloro-1-phenyl-3-chloromethyl-2(1H)-quinolone with sodium triazole in DMF. Chromatograph to obtain the major product, 1-phenyl-7-chloro-3-(1H-1,2,4-triazol-1-ylmethyl)-2(1H)-quinolone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05318971 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-7d455a825aa44506a65ff779b87cdd04 |
| Source note | uspto-grants-1994_06 |