6639-66-3 → HCID 19021693, compound

HRID 1108990Notes

Reaction equation

HRID 1108990 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][C:11]=1[O:12][CH2:13][O:14][CH3:15])[C:8](=O)[CH2:7][CH2:6]2.CC1C=CC(N=[CH:25][C:26]2[C:27]([NH2:35])=[CH:28][C:29]3[O:33][CH2:32][O:31][C:30]=3[CH:34]=2)=CC=1>>[CH3:15][O:14][CH2:13][O:12][C:11]1[C:3]([O:2][CH3:1])=[CH:4][C:5]2[CH2:6][C:7]3[C:8]([C:9]=2[CH:10]=1)=[N:35][C:27]1[CH:28]=[C:29]2[O:33][CH2:32][O:31][C:30]2=[CH:34][C:26]=1[CH:25]=3

Participants

3

Reactant 2

HCID 2416176639-66-3HCID 190216895-Methoxy-6-(methoxymethoxy)-2,3-dihydro-1H-inden-1-one

Product 1

HCID 19021693HCID 19021693, compound

Procedure

Using the procedure of Example 1, 5-methoxy-6-methoxymethoxyindan-1-one (452 mg, 2.03 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (517 mg, 2.03 mmol) to yields 7-methoxymethoxy-8-methoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline. This material is used directly in part (B) without further isolation or purification except for the few milligrams need for NMR and mass spectral studies.

Sources & evidence

ORD record
ord-9893c7c685aa44e48fcc4fcc85bca400
Source dataset
uspto-grants-1994_06
Patent number
US05318976

Reaction notes

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