HuagongsheHuagongshe Chemistry Print Report · For research reference only
6639-66-3 → HCID 19021693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6639-66-3 | HCID 241617 | — |
| Reactant | 5-Methoxy-6-(methoxymethoxy)-2,3-dihydro-1H-inden-1-one | HCID 19021689 | — |
| Product | HCID 19021693 | HCID 19021693 | — |
Reaction Steps
Using the procedure of Example 1, 5-methoxy-6-methoxymethoxyindan-1-one (452 mg, 2.03 mmol) is reacted with 6[[(4-methylphenyl)imino]methyl]-1,3-benzodioxol-5-amine (517 mg, 2.03 mmol) to yields 7-methoxymethoxy-8-methoxy-10H-1,3-dioxolo[4,5-g]indeno[1,2-b]quinoline. This material is used directly in part (B) without further isolation or purification except for the few milligrams need for NMR and mass spectral studies.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05318976 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-9893c7c685aa44e48fcc4fcc85bca400 |
| Source note | uspto-grants-1994_06 |