HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54470755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3,5-Di-tert-butyl-4-hydroxybenzaldehyde | HCID 73219 | — |
| Reactant | HCID 19022088 | HCID 19022088 | — |
| Product | HCID 54470755 | HCID 54470755 | 46.4% |
Reaction Steps
Substantially in the same manner as in Example 39 (3), 8.31 g of the thus obtained {1-(N-dimethylaminocarbamoyl)-2-oxopyrrolidin-3-yl}phosphonium bromide, 3.79 g (16.2 mmol) of 3,5-di-tert-butyl-4-hydroxybenzaldehyde and 4.51 ml (32.4 mmol) of triethylamine were treated to give 2.91 g of the objective compound (Ia-26) in 46.4% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05319100 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-0dbc81bbcde74beeae65edcb581e1229 |
| Source note | uspto-grants-1994_06 |