Hydrochloric Acid → 4-Hydroxyphenylglyoxal

HRID 1109313Notes

Reaction equation

HRID 1109313 reaction equation
N([O-])=[O:2].[Na+].Cl.[CH3:6][C:7]([C:9]1[CH:10]=[CH:11][C:12]([OH:15])=[CH:13][CH:14]=1)=[O:8]>O>[OH:15][C:12]1[CH:13]=[CH:14][C:9]([C:7]([CH:6]=[O:2])=[O:8])=[CH:10][CH:11]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 74694'-HydroxyacetophenoneHCID 23668193Sodium Nitrite

Product 1

HCID 905684-Hydroxyphenylglyoxal

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

adding sodium nitrite and hydrochloric acid to a solution of 4-hydroxyacetophenone in water to form 4-hydroxyphenylglyoxal;

Sources & evidence

ORD record
ord-630c5e0dd31a48bab30ce90082f08969
Source dataset
uspto-grants-1994_06
Patent number
US05319142

Reaction notes

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