HRID1109430
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
After 1.2 g of 4'-n-nonyloxybiphenyl-4-carboxylic acid was heated together with an excess amount of thionyl chloride for 6 hours under a reflux condition, unaltered thionyl chloride was distilled off to obtain 1.25 g of 4'-n-nonyloxybiphenyl-4-carboxylic acid chloride.
WORKUP
后处理
- distillationwas distilled off