化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 4'-n-Nonyloxybiphenyl-4-carboxylic acid chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4'-(Nonyloxy)[1,1'-biphenyl]-4-carboxylic acid | HCID 3620263 | — |
| 生成物 | 4'-n-Nonyloxybiphenyl-4-carboxylic acid chloride | HCID 12080273 | — |
反応手順
After 1.2 g of 4'-n-nonyloxybiphenyl-4-carboxylic acid was heated together with an excess amount of thionyl chloride for 6 hours under a reflux condition, unaltered thionyl chloride was distilled off to obtain 1.25 g of 4'-n-nonyloxybiphenyl-4-carboxylic acid chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05320776 |
| 出典データセット | uspto-grants-1994_06 |
| ORD ID | ord-b75ec5e9a4644b7d97f746bc7a0b9d13 |
| 出典メモ | uspto-grants-1994_06 |