(Chloromethyl)cyclopropane → HCID 19020663, compound

HRID 1109493Notes

Reaction equation

HRID 1109493 reaction equation
[CH:1]1([CH2:4][N:5]2[C:14](=[O:15])[C:13]3[NH:12][CH:11]=[N:10][C:9]=3[N:8]([CH2:16][CH:17]3[CH2:19][CH2:18]3)[C:6]2=[O:7])[CH2:3][CH2:2]1.[CH:20]1([CH2:23]Cl)[CH2:22][CH2:21]1>>[CH:1]1([CH2:4][N:5]2[C:14](=[O:15])[C:13]3[N:12]([CH2:23][CH:20]4[CH2:22][CH2:21]4)[CH:11]=[N:10][C:9]=3[N:8]([CH2:16][CH:17]3[CH2:19][CH2:18]3)[C:6]2=[O:7])[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 80013(Chloromethyl)cyclopropaneHCID 152913031,3-Dicyclopropylmethyl xanthine

Product 1

HCID 19020663HCID 19020663, compound

Procedure

1,3-Tri-cyclopropylmethyl-xanthine was prepared from 1,3-di-cyclopropylmethyl xanthine and cyclopropylchloromethane using an analogous procedure to that described in Example 5. The title compound was isolated as a crystalline solid, m.p. 78° C.

Sources & evidence

ORD record
ord-62561b09262f4c1dad5b16282f8eb62b
Source dataset
uspto-grants-1994_06
Patent number
US05321029

Reaction notes

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