HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 19020657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Cyclohexane, (bromomethyl)- | HCID 137636 | — |
| Reactant | HCID 19020648 | HCID 19020648 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19020657 | HCID 19020657 | — |
Reaction Steps
The title compound was prepared by stirring 1-cyclopropylmethyl-7-(3-oxobutyl)xanthine, 5 g, with 4.6 mls of bromomethylcyclohexane and 5.2 g of potassium carbonate in 30 ml DMF over 5 hours. After evaporation of the solvent the title compound was purified by column chromatography (ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05321029 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-3c83bc80f7194cb2b8d3f6a2d497b244 |
| Source note | uspto-grants-1994_06 |