HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminophenol → HCID 19019453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminophenol | HCID 403 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19019453 | HCID 19019453 | — |
Reaction Steps
To a stirred mixture of 50.2 g of p-hydroxyaniline and 38.7 g of sodium bicarbonate in 1.5 1 of ethanol was added dropwise 73 g of 3-nitro-4-chloropyridine in 2.0 l of ethanol. After stirring overnight at room temperature, the resulting solids were filtered, washed with water (2 l) and dried, 85.4 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05322847 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-41b80e5f9d904910a10ef2bd29c76d67 |
| Source note | uspto-grants-1994_06 |