HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-[(E)-2-(7-Chloroquinolin-2-yl)ethenyl]benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Isophthalaldehyde | HCID 34777 | — |
| Reactant | 7-Chloro-2-methylquinoline | HCID 138395 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 3-[(E)-2-(7-Chloroquinolin-2-yl)ethenyl]benzaldehyde | HCID 10017305 | 52% |
Reaction Steps
Starting with 6.56 g of 2-methyl-7-chloroquinoline, 10.4 ml of acetic anhydride and 4.95 g of isophthalaldehyde in 100 ml of xylene and using the procedure of Preparation Il, there was obtained 5.64 g of the desired product as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05322847 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-85170f90796849a9ba10f2d9e0e9a308 |
| Source note | uspto-grants-1994_06 |