huagongshe.com
HRID1109770

反应详情

EQUATION

反应方程式

HRID 1109770 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：O=Cc1cccc(C=O)c1
HCID34777

1,3-Benzenedicarboxaldehyde

C8H6O2

结构：Cc1ccc2ccc(Cl)cc2n1
HCID138395

7-Chloro-2-methylquinoline

C10H8ClN

PRODUCTS

生成物

1
结构：O=Cc1cccc(/C=C/c2ccc3ccc(Cl)cc3n2)c1
HCID10017305

3-[(E)-2-(7-Chloroquinolin-2-yl)ethenyl]benzaldehyde

C18H12ClNO

收率 52%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

Starting with 6.56 g of 2-methyl-7-chloroquinoline, 10.4 ml of acetic anhydride and 4.95 g of isophthalaldehyde in 100 ml of xylene and using the procedure of Preparation Il, there was obtained 5.64 g of the desired product as a yellow solid.

WORKUP

后处理

  1. customthe procedure of Preparation Il