HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 9904687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Sodium Phosphate, Dibasic | HCID 24203 | — |
| Reactant | HCID 178504907 | HCID 178504907 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9904687 | HCID 9904687 | — |
Reaction Steps
For example, (2S,4R)-1-p-nitrobenzyloxycarbonyl -4-methanesulfonyl-2-pyrrolidinethiocarboxylic acid is allowed to react with disodium hydrogenphosphate or triethylamine in methylene chloride or tetrahydrofuran, thereby to give (1S,4S)-5-p-nitrobenzyloxycarbonyl-2-thia-5-azabicyclo[2.2.1]heptan-3-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05322952 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-2665c7cbce56476595827e08561e3fcd |
| Source note | uspto-grants-1994_06 |