Chlorosuccinimide → HCID 19019911, compound

Participants

Reaction Steps

Dimethyl 4-chloro-3,6-dihydrophthalate (1.1 g) and N-chlorosuccinimide (0.6 g) in methylene chloride (4.1 g) was added to pyridinium poly(hydrogen fluoride) (3.1 g) at room temperature. The reaction mixture was stirred at room temperature for 2 hours. The reaction mixture was carefully poured into methylene chloride containing solid sodium carbonate. The methylene chloride layer was filtered and dried with magnesium sulfate and the solvent removed under reduced pressure.

Provenance & Evidence