反应详情

Durene was dissolved in benzene to give a molar ratio of benzene/durene of 2.2. The solution was pumped into the micro-reactor and loaded with 0.50 g of the same Fe-Mo-DBH catalyst used in Example 29 and oxidized in a flow of premixed gas consisting of 6 vol % O2 and 6 vol % N2 in He at two different temperatures, 425° C. and 450° C. Product effluent was analyzed by GC, and each product identified with GC/MS. Results are summarized in Table 23 below