Hydrochloric Acid → HCID 131718521, compound

HRID 1110033Notes

Reaction equation

HRID 1110033 reaction equation
[ClH:1].C([C:9]1[N:19]2[C:20]3[C:15]([CH2:16][CH2:17][CH2:18]2)=[CH:14][CH:13]=[CH:12][C:11]=3[C:10]=1CCN1CCN(C2C=C(C)C=CN=2)CC1)C1C=CC=CC=1>>[ClH:1].[ClH:1].[CH:10]1[C:11]2=[C:20]3[C:15](=[CH:14][CH:13]=[CH:12]2)[CH2:16][CH2:17][CH2:18][N:19]3[CH:9]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 10478944HCID 10478944, compound

Product 1

HCID 131718521HCID 131718521, compound

Procedure

The title base obtained above was converted into the corresponding hydrochloride as described in Example 13C). 1.5 g of 2-benzyl-5,6-dihydro-1-{2-[4-(4-methylpyridin-2-yl)-piperazin-1-yl]ethyl}-4H-pyrrolo[3,2,1-ij]quinoline.2.4 HCl 2 H2O were obtained as a pale grey powder having a melting point of 186°-208° C.

Sources & evidence

ORD record
ord-590d978f845b41cd86178de05f7dffc3
Source dataset
uspto-grants-1994_06
Patent number
US05324725

Reaction notes

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