P-Toluenesulfonylhydrazide → HCID 70358998, compound

Participants

Reaction Steps

A mixture of 5.00 g (31 mmol, Aldrich) of 5-methoxy-1-indanone and 6.33 g (34.0 mmol, Aldrich) of p-toluenesulfonhydrazide in 50 ml EtOH was heated on a steam bath until homogeneous. The solution was cooled and the solid which formed was filtered to yield 10.05 g (99%) of title compound as cream colored crystals: m.p. 195°-196° C.

Provenance & Evidence