HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-2-(2-((tert-Butoxycarbonyl)amino)propanamido)acetic acid → Boc-Gly-Phe-Gly-Val-Gly-Ala-Gly-Val-Pro-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-2-(2-((tert-Butoxycarbonyl)amino)propanamido)acetic acid | HCID 192414 | — |
| Reactant | Boc-Gly-Phe-Gly-Val-Gly-Ala-Gly-Val-Pro-OBzl | HCID 131715253 | — |
| Product | Boc-Gly-Phe-Gly-Val-Gly-Ala-Gly-Val-Pro-OH | HCID 131715256 | — |
Reaction Steps
The above peptide XV was hydrogenated as described for the preparation VIII to obtain the product in quantitative yield. Rf3 0.22. Anal. calcd. for C40H61N9O12:C 55.66, H 7.12, N 14.60%. Found: C 55.86, H 7.23, N 14.14%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04976734 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-30dc1d449a2247ffb4e2b521972541e5 |
| Source note | uspto-grants-1990_12 |