Hydrochloric Acid → HCID 15052635, compound

HRID 1110992Notes

Reaction equation

HRID 1110992 reaction equation
C[O:2][C:3](=[O:20])[C@H:4]([CH2:11][C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=1)[NH:5][C:6]([N:8]([CH3:10])[CH3:9])=[O:7].Cl>>[CH3:10][N:8]([CH3:9])[C:6]([NH:5][C@H:4]([C:3]([OH:20])=[O:2])[CH2:11][C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=1)=[O:7]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 18632657HCID 18632657, compound

Product 1

HCID 15052635HCID 15052635, compound

Procedure

Prepared according to the procedure of Example 56 from the resultant compound of Example 57 with the modification that the product was isolated by pouring the reaction mixture into 2M HCl and extracting with ethyl acetate which was dried over Na2SO4 and evaporated. EI-MS: M+ =266.

Workup

  1. customPrepared
  2. customwas isolated
  3. extractionextracting with ethyl acetate which
  4. dry with materialwas dried over Na2SO4
  5. customevaporated

Sources & evidence

ORD record
ord-e001218114f24b86bd31ba2adeca2d1c
Source dataset
uspto-grants-1990_12
Patent number
US04977277

Reaction notes

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