HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19768448, compound → HCID 19768452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19768448 | HCID 19768448 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19768452 | HCID 19768452 | — |
Reaction Steps
A solution of N-[1-[1,6-dihydro-6-oxo-1-(phenylmethyl)-3-pyridinyl]-cyclohexyl]formamide hydrochloride (13.4 g) in 200 ml of methanol was heated at reflux for 17 hours. The mixture was cooled, and the resultant crystals were collected, affording 5.6 g of analytically pure 5-(1-aminocyclohexyl)-1-(phenylmethyl)-2(1H)-pyridinone hydrochloride, m.p. 248°-250° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978663 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-baabad889ec74c17985bdd30a8206b44 |
| Source note | uspto-grants-1990_12 |