HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15137052, compound → HCID 15137043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15137052 | HCID 15137052 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15137043 | HCID 15137043 | 100% |
Reaction Steps
A suspension of 0.250 g (1.02 mmol) of the product of Example 12, Step I and 50 mg of 5% Pd/C in 5 mL of ethyl acetate was shaken under 40 psi H2 for 1 h. The solution was filtered through Celite and the filtrate was concentrated to afford 0.250 g (100%) of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978679 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-3123a24972224296a58819a6035d29cb |
| Source note | uspto-grants-1990_12 |