HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl propiolate → HCID 15079747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl propiolate | HCID 13536 | — |
| Reactant | HCID 15079736 | HCID 15079736 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15079747 | HCID 15079747 | — |
Reaction Steps
In the manner given in Example 1, 2-amino-7-cyano-5-(p-methylsulfonylphenyl)-3H-1,4-benzodiazepine, methyl propiolate and methanol were refluxed. The mixture was chromatographed to give 9-cyano-7-(p-methylsulfonylphenyl)pyrimido[1,2-a][1,4]benzodiazepin-3(5H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978753 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-a05acfd4be6a439ca263726d234a34cb |
| Source note | uspto-grants-1990_12 |