HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl propiolate → HCID 15079749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl propiolate | HCID 13536 | — |
| Reactant | HCID 15079779 | HCID 15079779 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15079749 | HCID 15079749 | — |
Reaction Steps
In the manner given in Example 2, 2-amino-7-chloro-5-(2,6-difluorophenyl)-3H-1,4-benzodiazepine, methyl propiolate and methanol were refluxed. The mixture was chromatographed to give 9-chloro-7-(2,6-difluorophenyl)pyrimido[1,2-a][1,4]benzodiazepin-3(5H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978753 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-6765dbc809184e06a43d96ecb1e16cc8 |
| Source note | uspto-grants-1990_12 |