HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 22153698, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 15079755 | HCID 15079755 | — |
| Reactant | tetrahydrofuran N,N-dimethylformamide | HCID 21974620 | — |
| Reactant | HCID 22153717 | HCID 22153717 | — |
| Product | HCID 22153698 | HCID 22153698 | — |
Reaction Steps
In the manner given in Example 21, carbonyldiimidazole, 6-(4-methylpiperazinyl)-2-hexynoic acid, and 2-amino-6-methoxy-5-(o-fluorophenyl)-3H-1,4-benzodiazepine was stirred in tetrahydrofuran-dimethylformamide to give 8-methoxy-1-[1-(4-methylpiperazinyl)propyl]-7-(o-fluorophenyl)pyrimido[1,2-a][1,4]benzodiazepin-3(5H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978753 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-6ad5efa9aca14c03b9997d1e94510446 |
| Source note | uspto-grants-1990_12 |