HRID1111219

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID66321

Lithium iodide

ILi

结构：CCOC(=O)c1cc(=O)nc2n1-c1ccc(Cl)cc1C(c1ccccc1Cl)=NC2

HCID15079786

未命名化合物

PRODUCTS

生成物

结构：O=c1ccn2c(n1)CN=C(c1ccccc1Cl)c1cc(Cl)ccc1-2

HCID15079804

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

In the manner given in Example 32, 1-carboethoxy-9-chloro-7-(o-chlorophenyl)pyrimido[1,2-a][1,4]benzodiazepin-3(5H)-one was heated in pyridine with lithium iodide to give 9-chloro-7-(o-chlorophenyl)pyrimido[1,2-a][1,4]benzodiazepin-3(5H)-one.