HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Bromide → 1,1-Ethanediol, 1,1-diacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Bromide | HCID 6323 | — |
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1,1-Ethanediol, 1,1-diacetate | HCID 222536 | 36,567.602% |
Reaction Steps
The procedure of Example 9 was repeated except that 10 g of methyl bromide was used in place of methyl iodide and the reaction was effected for 6 hours. GC analysis showed that 0.212 g of vinyl acetate and 65.8 g of ethylidene diacetate were formed with considerable amount of acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978778 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-0b7fc084fffb4863a4fbf122954b1f1a |
| Source note | uspto-grants-1990_12 |