HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-Aminoundecanoic acid → Undecanoic acid, 11-(((2-benzoyl-4-chlorophenyl)sulfonyl)amino)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-Aminoundecanoic acid | HCID 17083 | — |
| Reactant | 2-benzoyl-4-chloro-benzenesulfonyl Chloride | HCID 2756600 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | Undecanoic acid, 11-(((2-benzoyl-4-chlorophenyl)sulfonyl)amino)- | HCID 3086745 | — |
Reaction Steps
24.16 g (0.12 mole) of 11-aminoundecanoic acid in 250 ml of normal caustic soda are added to 37.9 g (0.12 mole) of 2-benzoyl-4-chlorobenzenesulphonyl chloride in 250 ml of methylene chloride, at 0° C. and with stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04980349 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-4505addb61684dd8afadb83d7b71bb05 |
| Source note | uspto-grants-1990_12 |