HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 6-(2-Benzoyl-4-chlorobenzenesulphonamido)-capronitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-Aminohexanenitrile | HCID 17079 | — |
| Reactant | 2-benzoyl-4-chloro-benzenesulfonyl Chloride | HCID 2756600 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 6-(2-Benzoyl-4-chlorobenzenesulphonamido)-capronitrile | HCID 54210096 | — |
Reaction Steps
15 ml of redistilled triethylamine are added to 15.7 g of 4-chloro-2-benzoylbenzenesulphonyl chloride in 100 ml of anhydrous dichloromethane, and 5.6 g of 6-aminocapronitrile in 20 ml of dichloromethane are then added dropwise at 0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04980349 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-23516ffe816449acb98d3a0a33b39b85 |
| Source note | uspto-grants-1990_12 |