Carbon Disulfide → HCID 178444348, compound

Participants

Reaction Steps

A solution of 390 mg of p-[trans-4-(trans-1-pentenyl)cyclohexyl]aniline (purity 93%) in 4 ml of hexane was treated successively with 446 μl of triethylamine and 214 μl of carbon disulphide and the mixture was then left to stand at 0° C. for 65 hours. The yellow precipitate obtained was filtered off, washed twice with hexane and dried in a high vacuum. There were obtained 428 mg of triethylammonium p-[trans 4-(trans-1-pentenyl)cyclohexyl]phenyldithiocarbamate which was processed directly without additional purification.

Provenance & Evidence