Hydrochloric Acid → HCID 86736054, compound

HRID 1111730Notes

Reaction equation

HRID 1111730 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH:8]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][N:13]=2)[C:9]([NH2:11])=[S:10])[CH2:3][CH2:2]1.[ClH:18]>CCOCC>[ClH:18].[ClH:18].[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH:8]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][N:13]=2)[C:9]([NH2:11])=[S:10])[CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 53838371HCID 53838371, compound

Product 1

HCID 86736054HCID 86736054, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

3Morpholino-2-(2-pyridyl)thiopropanamide (500 mg.) in ether is added to ethereal hydrogen chloride. The precipitate is filtered off and washed with ether to give 3-morpholino-2-(2-pyridyl)thiopropanamide dihydrochloride.

Workup

  1. filtrationThe precipitate is filtered off
  2. washwashed with ether

Sources & evidence

ORD record
ord-1a46f6a4a9a34764982e2c0c8a16bf09
Source dataset
uspto-grants-1978_10
Patent number
US04118567

Reaction notes

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