HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethanol → 2-Chloroethyl 2-(4-chlorophenoxy)-2-methylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethanol | HCID 34 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Clofibric Acid | HCID 2797 | — |
| Product | 2-Chloroethyl 2-(4-chlorophenoxy)-2-methylpropionate | HCID 104099 | — |
Reaction Steps
107.3 g (0.5 mole) of p-chlorophenoxy-2-methylpropionic acid are dissolved in 241.5 g (3 moles) of 2-chloroethanol. The solution is saturated with HCl gas. The excess of solvent is distilled under 11 Torr. The ester is distilled under 0.02 Torr, at a temperature of 97°-98°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118583 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-5a954809def746cda2a29a76c1b5ad42 |
| Source note | uspto-grants-1978_10 |