HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethanol → HCID 53916271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethanol | HCID 34 | — |
| Reactant | Salicylic Acid | HCID 338 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 53916271 | HCID 53916271 | — |
Reaction Steps
A solution of 13.8 g (0.1 mole) of salicylic acid in 48.3 g (0.6 mole) of 2-chloro-ethanol in the presence of 4 ml of sulfuric acid is heated to 110° for 2 hours. After removing the excess of 2-chloro-ethanol, the ether solution of the product is extracted with an aqueous solution of 5% CO3HNa. The ether is removed and the product is distilled. B.p.: 128°-129°/11 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118583 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-15b3d135325e44ce8d451bf03ed7f45c |
| Source note | uspto-grants-1978_10 |