HRID1111816

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID53167

1-Methylpiperazine

C5H12N2

$结构：O=C([O-])/C=C\C(=O)[O-]$

HCID5288227

Maleate (2-)

C4H2O4-2

HCID12765115

2-Chlorodibenzo[b,f]oxepin-10(11H)-one

C14H9ClO2

结构：CN1CCN(C2=Cc3cc(Cl)ccc3Oc3ccccc32)CC1

HCID12765116

未命名化合物

PRODUCTS

生成物

结构：CN1CCN(C2Cc3cc(Cl)ccc3Oc3ccccc32)CC1.Cl.Cl

HCID22767837

未命名化合物

PROCEDURE

实验过程

The 1-[2-chloro-dibenz[b,f]oxepin-10-yl]-4-methyl-piperazine having a melting point of 119°-120° C. [maleate: melting point 200°-202° C. (with decomposition)]used as the starting material can be prepared in an analogous manner to that described in Example 14 from 2-chloro-10,11-dihydro-dibenz[b,f]oxepin-10-one and 1-methyl-piperazine.

WORKUP

后处理

customcan be prepared in an analogous manner to that