HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloro-4-nitrobenzene → HCID 22765592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloro-4-nitrobenzene | HCID 7443 | — |
| Reactant | Sodium benzenethiolate | HCID 4110039 | — |
| Product | HCID 22765592 | HCID 22765592 | 31% |
Reaction Steps
The procedure was as previously mentioned using 1-nitro-3,4-dichlorobenzene (10 g, 0.052 M) and sodium thiophenoxide (13.75 g, 0.104 M). mp = 97°-101°. Yield 31%. The reaction product was characterized by NMR, 13CNMR, ir, and Mass Spectra (M+ = 339).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04119629 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-8f577ca5c6d446658eebac02006fdba0 |
| Source note | uspto-grants-1978_10 |