3,5-Dichloroaniline → HCID 22765796, compound

HRID 1111885Notes

Reaction equation

HRID 1111885 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[C:7]([Cl:9])[CH:8]=1)[NH2:5].[C:10](OCC)(OCC)([O:13][CH2:14][CH3:15])[CH2:11][CH3:12]>>[Cl:1][C:2]1[CH:3]=[C:4]([N:5]=[C:10]([O:13][CH2:14][CH3:15])[CH2:11][CH3:12])[CH:6]=[C:7]([Cl:9])[CH:8]=1

Participants

3

Reactant 2

HCID 122813,5-DichloroanilineHCID 66995Ethyl orthopropionate

Product 1

HCID 22765796HCID 22765796, compound

Procedure

This is prepared by the reaction of equimolar amounts of 3,5-dichloroaniline and triethyl orthopropionate, as generally described in Chemical Reviews 61, 185 (1961), to give an 86% weight yield of product distilling at 89° C./0.15 mm.

Workup

  1. customto give an 86% weight yield of product
  2. distillationdistilling at 89° C./0.15 mm

Sources & evidence

ORD record
ord-bb20b7de18b24e16a765fc2e17fc4e6d
Source dataset
uspto-grants-1978_10
Patent number
US04119667

Reaction notes

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