Hydrochloric Acid → HCID 13355696, compound
Reaction equation
Cl.[NH2:2][C:3]1[C:8]([C:9]#[N:10])=[CH:7][C:6]([C:11](=[O:19])[CH2:12][NH:13][C:14]([CH2:17][CH3:18])([CH3:16])[CH3:15])=[CH:5][C:4]=1[C:20]#[N:21]>>[NH2:2][C:3]1[C:4]([C:20]#[N:21])=[CH:5][C:6]([CH:11]([OH:19])[CH2:12][NH:13][C:14]([CH2:17][CH3:18])([CH3:16])[CH3:15])=[CH:7][C:8]=1[C:9]#[N:10]Participants
3
Procedure
m.p. of the hydrochloride: 231°-233° C. (decomp.), was prepared from 4'-amino-3',5'-dicyano-2-tert.pentylamino-acetophenone analogous to Example 48.
Sources & evidence
- ORD record
- ord-8ddf7ee750b84ed9aac4c3211fa0ba1d
- Source dataset
- uspto-grants-1978_10
- Patent number
- US04119710
Reaction notes
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