HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 22765156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 3-(2-Chloroethanesulfonyl)-N-[2-(ethenylsulfanyl)ethyl]propanamide | HCID 22765149 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22765156 | HCID 22765156 | — |
Reaction Steps
A suspension of 6 g Intermediate 2 in 25 ml acetic acid was treated at 20° C. with 2.5 ml of 30 % hydrogen peroxide and 3 ml acetic acid. After 2 hours the solution was evaporated and the residue stirred with ether. The solid was filtered, dried and recrystallised from ethanol-petrolether. Yield 4.85 g; Mp. 108° to 109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120898 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-e459a77a6f2043d4b7b9f1eb0f6bbedb |
| Source note | uspto-grants-1978_10 |