HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 22765159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 22765154 | HCID 22765154 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22765159 | HCID 22765159 | — |
Reaction Steps
4.05 g Intermediate 6 in 20 ml acetic acid was oxidised with 30 % hydrogen peroxide in the usual way. After 2 hours, the solution was evaporated and the residue stirred with ether. The solidified product was filtered off and recrystallised from ethanolpetrolether. Yield 3.1 g; Mp. 113° to 135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120898 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-1b12998c522749f09485c9136719f997 |
| Source note | uspto-grants-1978_10 |