HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 22765342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 5(2-Hydroxy-3-tert.-butylaminopropoxy)-1-oxo-2-methyl-1,2-dihydro-beta-carboline acetate | HCID 86736070 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22765342 | HCID 22765342 | — |
Reaction Steps
The above-obtained base is dissolved in about 50 ml. methanol and mixed with 0.8 ml. glacial acetic acid. After the addition of about 50 ml. diethyl ether, a precipitate is slowly formed. This is filtered off with suction and dried to give 2.6 g. 5(2-hydroxy-3-tert.-butylaminopropoxy)-1-oxo-2-methyl-1,2-dihydro-β-carboline acetate; m.p. 221°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04120963 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-239b179aad824d488afcc0d1383013bd |
| Source note | uspto-grants-1978_10 |