Vincamine → Vincamine caprate

HRID 1112374Notes

Reaction equation

HRID 1112374 reaction equation
[CH3:1][CH2:2][C@:3]12[CH2:19][C@:18]([OH:24])([C:20]([O:22][CH3:23])=[O:21])[N:17]3[C:9]4=[C:10]([CH2:25][CH2:26][N:7]([C@@H:8]14)[CH2:6][CH2:5][CH2:4]2)[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=13>O>[CH3:1][CH2:2][C@:3]12[CH2:19][C@:18]([OH:24])([C:20]([O:22][CH3:23])=[O:21])[N:17]3[C:9]4=[C:10]([CH2:25][CH2:26][N:7]([C@@H:8]14)[CH2:6][CH2:5][CH2:4]2)[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=13.[O-:22][C:20]([CH2:18][CH2:19][CH2:3][CH2:8][CH2:9][CH2:10][CH2:11][CH2:16][CH3:15])=[O:21]

Participants

3

Reactant 1

HCID 15376Vincamine

Product 1

HCID 86736097Vincamine caprate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

From 7.08 g (2.10-2 moles) of vincamine and 3.45 g (2.10-2 moles) of capric acid, there are obtained 10 g of an oily, semi-solid substance, insoluble in water and in the common organic solvents. The vincamine content is 65.3%.

Sources & evidence

ORD record
ord-c7c0c6bafb324704bc86cbf150465da7
Source dataset
uspto-grants-1978_10
Patent number
US04122179

Reaction notes

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