反应详情

The procedure as described in Example 1 was followed using phenacyl alcohol and butylcyanamide. A colourless oil was obtained after distillation of the product. Wt. = 5.0 g., 47% Yield. b.p. 134° C/0.1 mm., which crystallised on standing. The analytical sample which separated as needles from petrol (40°-60° C) had m.p. 52°-53° C.

1. customA colourless oil was obtained
2. distillationafter distillation of the product
3. custom, which crystallised
4. customThe analytical sample which separated as needles from petrol (40°-60° C)