HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Hydroxyacetophenone → 2-(N-Butylamino)-4-phenyloxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Hydroxyacetophenone | HCID 68490 | — |
| Reactant | Butylcyanamide | HCID 12295218 | — |
| Product | 2-(N-Butylamino)-4-phenyloxazole | HCID 12295238 | 47% |
Reaction Steps
The procedure as described in Example 1 was followed using phenacyl alcohol and butylcyanamide. A colourless oil was obtained after distillation of the product. Wt. = 5.0 g., 47% Yield. b.p. 134° C/0.1 mm., which crystallised on standing. The analytical sample which separated as needles from petrol (40°-60° C) had m.p. 52°-53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04122183 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-8852b30e462e458da452a7751c0dfa92 |
| Source note | uspto-grants-1978_10 |