HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 2-(3-Morpholin-4-YL-propoxy)-benzaldehyde | HCID 13795260 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20394050 | 76.5% |
Reaction Steps
2-[3-(4-Morpholinyl)propoxy]benzaldehyde (31.7g) is reacted with 15.8g of phenethylamine in 130 ml of toluene following the procedure described in Example 1A to yield 34.3g of product as an oil, boiling point 215°-219° C at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04122255 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-da899c30bccc4b958efefe2f136049f3 |
| Source note | uspto-grants-1978_10 |