HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methyl]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20394050 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methyl]benzeneethanamine | HCID 21322756 | — |
Reaction Steps
N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]-benzeneethanamine (17g) is reduced with 5.4g of sodium borohydride in 85 ml of methanol following the procedure described in Example 1B to yield 12.8g of product as an oil, boiling point 219°-223° C at 0.1-0.2 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04122255 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-5339cb7e8d0e41b4b42a02452c167729 |
| Source note | uspto-grants-1978_10 |