2-Chlorobenzyl chloride → HCID 70620802, compound

HRID 1112467Notes

Reaction equation

HRID 1112467 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[S:13][C:8]3([NH:12][CH2:11][CH2:10][NH:9]3)[C:6]=2[CH:7]=1.[Cl:14][C:15]1[CH:22]=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17]Cl>CO>[ClH:1].[Cl:14][C:15]1[CH:22]=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17][S:13][C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][C:6]=1[C:8]1[NH:12][CH2:11][CH2:10][N:9]=1

Participants

4

Reactant 2

HCID 119062-Chlorobenzyl chlorideHCID 704691194-Chlorobenzothietane-2-spiro-2'-imidazoline

Product 1

HCID 70620802HCID 70620802, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

32 Parts of 4-chlorobenzothietane-2-spiro-2'-imidazoline is reacted with 26 parts of 2-chlorobenzyl chloride in 300 parts of methanol. The yield is 52 parts (90% of theory) and the melting point is 260° C. with decomposition.

Sources & evidence

ORD record
ord-8f40581397244e9184a7e75388e4d35a
Source dataset
uspto-grants-1978_10
Patent number
US04122263

Reaction notes

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